Environmental Process Analysis

Provides the basic skills and information required to prepare an environmental sample for analysis. Divided into two sections, i.e. Inorganic Analysis and Organic Analysis, this book covers selected techniques, principally atomic spectroscopy and chromatography. Using flow diagrams to augment the experimental information, it highlights the most appropriate methods and the likely results. Detailed experimental information provided in an easy-to-follow style with illustrations Describes the specific sample preparation approaches necessary to analyse a particular sample type Discussion of selected literature sources highlights the most appropriate methods and the likely results obtained

Tested and proven strategy to develop optimal automated process fault analyzers Process fault analyzers monitor process operations in order to identify the underlying causes of operational problems. Several diagnostic strategies exist for automating process fault analysis; however, automated fault analysis is still not widely used within the processing industries due to problems of cost and performance as well as the difficulty of modeling process behavior at needed levels of detail. In response, this book presents the method of minimal evidence (MOME), a model-based diagnostic strategy that facilitates the development and implementation of optimal automated process fault analyzers. MOME was created at the University of Delaware by the researchers who developed the FALCON system, a real-time, online process fault analyzer. The authors demonstrate how MOME is used to diagnose single and multiple fault situations, determine the strategic placement of process sensors, and distribute fault analyzers within large processing systems. Optimal Automated Process Fault Analysis begins by exploring the need to automate process fault analysis. Next, the book examines: Logic of model-based reasoning as used in MOME MOME logic for performing single and multiple fault diagnoses Fuzzy logic algorithms for automating MOME Distributing process fault analyzers throughout large processing systems Virtual SPC analysis and its use in FALCONEER IV Process state transition logic and its use in FALCONEER IV The book concludes with a summary of the lessons learned by employing FALCONEER IV in actual process applications, including the benefits of «intelligent supervision» of process operations. With this book as their guide, readers have a powerful new tool for ensuring the safety and reliability of any chemical processing system.

A comprehensive set of real-world environmental laboratory experiments This complete summary of laboratory work presents a richly detailed set of classroom-tested experiments along with background information, safety and hazard notes, a list of chemicals and solutions needed, data collection sheets, and blank pages for compiling results and findings. This useful resource also: Focuses on environmental, i.e., «dirty» samples Stresses critical concepts like analysis techniques and documentation Includes water, air, and sediment experiments Includes an interactive software package for pollutant fate and transport modeling exercises Functions as a student portfolio of documentation abilities Offers instructors actual samples of student work for troubleshooting, notes on each procedure, and procedures for solutions preparation.

An integrated approach to understanding the principles of sampling, chemical analysis, and instrumentation This unique reference focuses on the overall framework and why various methodologies are used in environmental sampling and analysis. An understanding of the underlying theories and principles empowers environmental professionals to select and adapt the proper sampling and analytical protocols for specific contaminants as well as for specific project applications. Covering both field sampling and laboratory analysis, Fundamentals of Environmental Sampling and Analysis includes: A review of the basic analytical and organic chemistry, statistics, hydrogeology, and environmental regulations relevant to sampling and analysis An overview of the fundamentals of environmental sampling design, sampling techniques, and quality assurance/quality control (QA/QC) essential to acquire quality environmental data A detailed discussion of: the theories of absorption spectroscopy for qualitative and quantitative environmental analysis; metal analysis using various atomic absorption and emission spectrometric methods; and the instrumental principles of common chromatographic and electrochemical methods An introduction to advanced analytical techniques, including various hyphenated mass spectrometries and nuclear magnetic resonance spectroscopy With real-life case studies that illustrate the principles plus problems and questions at the end of each chapter to solidify understanding, this is a practical, hands-on reference for practitioners and a great textbook for upper-level undergraduates and graduate students in environmental science and engineering.

This book covers all aspects of environmental trace analysis from sampling through to preparation of the sample to the analytical techniques used to quantify the level of trace metals or organic compounds. The book is divided into two areas: sample preparation for inorganic analysis and sample preparation for organic analysis. This allows the reader to focus on key aspects related to the preparation of samples for their subsequent analysis. Selected case studies provide the reader with the opportunity to consider how the sample preparation approach can be optimized for their own area of expertise.

A COMPREHENSIVE TEXTBOOK AND REFERENCE FOR QUANTITATIVE ENVIRONMENTAL RISK ANALYSIS FOR BOTH CHEMICAL AND RADIOACTIVE CONTAMINANTS Environmental risk analysis is complex and interdisciplinary; this book explains the fundamental concepts and analytical methods in each essential discipline. With an emphasis on concepts and applications of quantitative tools plus coverage of analysis of both chemical and radioactive contaminants, this is a comprehensive resource. After an introduction and an overview of the basics of environmental modeling, the book covers key elements in environmental risk analysis methodology, including: Release assessment and source characterization Migration of contaminants in various media, including surface water, groundwater, the atmosphere, and the food chain Exposure assessment Basic human toxicology and dose-response Risk characterization, including dose-response modeling and analysis Risk management process and methods Risk communication and public participation This reference also relates risk analysis to current environmental laws and regulations. An ideal textbook for graduate students and upper-level undergraduates in various engineering and quantitative science disciplines, especially civil and environmental engineering, it is also a great reference for practitioners in industry, environmental consulting firms, and regulatory agencies.

This book focuses on plastics process analysis, instrumentation for modern manufacturing in the plastics industry. Process analysis is the starting point since plastics processing is different from processing of metals, ceramics, and other materials. Plastics materials show unique behavior in terms of heat transfer, fluid flow, viscoelastic behavior, and a dependence of the previous time, temperature and shear history which determines how the material responds during processing and its end use. Many of the manufacturing processes are continuous or cyclical in nature. The systems are flow systems in which the process variables, such as time, temperature, position, melt and hydraulic pressure, must be controlled to achieve a satisfactory product which is typically specified by critical dimensions and physical properties which vary with the processing conditions.  Instrumentation has to be selected so that it survives the harsh manufacturing environment of high pressures, temperatures and shear rates, and yet it has to have a fast response to measure the process dynamics. At many times the measurements have to be in a non-contact mode so as not to disturb the melt or the finished product. Plastics resins are reactive systems. The resins will degrade if the process conditions are not controlled. Analysis of the process allows one to strategize how to minimize degradation and optimize end-use properties.

Bayesian analysis of complex models based on stochastic processes has in recent years become a growing area. This book provides a unified treatment of Bayesian analysis of models based on stochastic processes, covering the main classes of stochastic processing including modeling, computational, inference, forecasting, decision making and important applied models. Key features: Explores Bayesian analysis of models based on stochastic processes, providing a unified treatment. Provides a thorough introduction for research students. Computational tools to deal with complex problems are illustrated along with real life case studies Looks at inference, prediction and decision making. Researchers, graduate and advanced undergraduate students interested in stochastic processes in fields such as statistics, operations research (OR), engineering, finance, economics, computer science and Bayesian analysis will benefit from reading this book. With numerous applications included, practitioners of OR, stochastic modelling and applied statistics will also find this book useful.

Still the only book offering comprehensive coverage of the analysis and design of both API equipment and ASME pressure vessels This edition of the classic guide to the analysis and design of process equipment has been thoroughly updated to reflect current practices as well as the latest ASME Codes and API standards. In addition to covering the code requirements governing the design of process equipment, the book supplies structural, mechanical, and chemical engineers with expert guidance to the analysis and design of storage tanks, pressure vessels, boilers, heat exchangers, and related process equipment and its associated external and internal components. The use of process equipment, such as storage tanks, pressure vessels, and heat exchangers has expanded considerably over the last few decades in both the petroleum and chemical industries. The extremely high pressures and temperatures involved with the processes for which the equipment is designed makes it potentially very dangerous to property and life if the equipment is not designed and manufactured to an exacting standard. Accordingly, codes and standards such as the ASME and API were written to assure safety. Still the only guide covering the design of both API equipment and ASME pressure vessels, Structural Analysis and Design of Process Equipment, 3rd Edition: Covers the design of rectangular vessels with various side thicknesses and updated equations for the design of heat exchangers Now includes numerical vibration analysis needed for earthquake evaluation Relates the requirements of the ASME codes to international standards Describes, in detail, the background and assumptions made in deriving many design equations underpinning the ASME and API standards Includes methods for designing components that are not covered in either the API or ASME, including ring girders, leg supports, and internal components Contains procedures for calculating thermal stresses and discontinuity analysis of various components Structural Analysis and Design of Process Equipment, 3rd Edition is an indispensable tool-of-the-trade for mechanical engineers and chemical engineers working in the petroleum and chemical industries, manufacturing, as well as plant engineers in need of a reference for process equipment in power plants, petrochemical facilities, and nuclear facilities.

A timely, hands-on guide to environmental issues and regulatory standards for the petroleum industry Environmental analysis and testing methods are an integral part of any current and future refining activities. Today's petroleum refining industry must be prepared to meet a growing number of challenges, both environmental and regulatory. Environmental Analysis and Technology for the Refining Industry focuses on the analytical issues inherent in any environmental monitoring or cleanup program as they apply to today's petroleum industry, not only during the refining process, but also during recovery operations, transport, storage, and utilization. Designed to help today's industry professionals identify test methods for monitoring and cleanup of petroleum-based pollutants, the book provides examples of the application of environmental regulations to petroleum refining and petroleum products, as well as current and proposed methods for the mitigation of environmental effects and waste management. Part I introduces petroleum technology, refining, and products, and reviews the nomenclature used by refiners, environmental scientists, and engineers. Part II discusses environmental technology and analysis, and provides information on environmental regulation and the impact of refining. Coverage includes: * In-depth descriptions of analyses related to gaseous emissions, liquid effluents, and solid waste * A checklist of relevant environmental regulations * Numerous real-world examples of the application of environmental regulations to petroleum refining and petroleum products * An analysis of current and proposed methods of environmental protection and waste management