Polyolefin Characterization

This guide to the properties and applications of polyolefin composites consolidates information to help the reader compare, select, and integrate a material solution as needed. It covers polyolefin microcomposites, polyolefin nanocomposites, and advanced polyolefin nano and molecular composites and discusses processing, morphological characterization, crystallization, structure and properties, and performance evaluation at micro and nano structural levels. It details modeling and simulation, engineering performance properties, and applications. This is a practical, hands-on reference for practicing professionals as well as graduate students.

The definitive reference on the properties and applications of polyolefin blends Polyolefins account for more than half of total plastics consumption in the world. In recent years, usage of and research on polyolefin blends have increased significantly due to new applications in medicine, packaging, and other fields and the development of novel polyolefins. With a special emphasis on nano- and micro-structures of crystals and phase morphology, Polyolefin Blends condenses and consolidates current information on polyolefins so that the reader can compare, select, and integrate a material solution. Focusing exclusively on the fundamental aspects as well as applications of polyolefin blends, this authoritative reference: * Features an introductory chapter that serves as a guide to polyolefin blends * Includes chapters covering formulation design, processing, characterization, modeling and simulation, engineering performance properties, and applications * Covers polyolefin/polyolefin blends and polyolefin/non-polyolefin blends * Discusses miscibility, phase behavior, functionalization, compatibilization, microstructure, crystallization, hierarchical morphology, and physical and mechanical properties * Covers new research trends including in-situ reactor blending and reactive processing, such as compatibilization/functionalization in the melt * Contains practical examples from open literature sources and commercial products With chapters contributed by leading experts from several countries, this is a must-have reference for scientists and engineers conducting research on polyolefin blends and for professionals in medical, packaging, and other commodity fields. It is also an excellent text for graduate students studying polymer science and polymer processing.

Monomers composed of carbon and hydrogen atoms are the simple building blocks that make up polyolefins – molecules which are extremely useful and which have an extraordinary range of properties and applications. How these monomer molecules are connected in the polymer chain defines the molecular architecture of polyolefins. Written by two world-renowned authors pooling their experience from industry and academia, this book adopts a unique engineering approach using elegant mathematical modeling techniques to relate polymerization conditions, reactor and catalyst type to polyolefin properties. Readers thus learn how to design and optimize polymerization conditions to produce polyolefins with a given microstructure, and how different types of reactors and processes are used to create the different products. Aimed at polymer chemists, plastics technologists, process engineers,the plastics industry, chemical engineers, materials scientists, and company libraries.

Introduces basic knowledge for nanomaterial characterization focusing on key properties and the different analytical techniques available Provides a quick reference to different analytical methods for a given property highlighting their pros and cons Presents numerous case studies, ranging from characterizing nanomaterials in coffee creamer suspension to measurement of airborne dust exposure levels Provides an introduction to other topics that are strongly related to nanomaterial characterization e.g. synthesis, reference material and metrology Includes state of the art techniques: scanning tunneling microscopy under extreme conditions, novel strategy for biological characterization and methods to visualize multidimensional characterization data

This book covers state-of-the-art techniques commonly used in modern materials characterization. Two important aspects of characterization, materials structures and chemical analysis, are included. Widely used techniques, such as metallography (light microscopy), X-ray diffraction, transmission and scanning electron microscopy, are described. In addition, the book introduces advanced techniques, including scanning probe microscopy. The second half of the book accordingly presents techniques such as X-ray energy dispersive spectroscopy (commonly equipped in the scanning electron microscope), fluorescence X-ray spectroscopy, and popular surface analysis techniques (XPS and SIMS). Finally, vibrational spectroscopy (FTIR and Raman) and thermal analysis are also covered.

This second volume in the series, “Sustainable Energy Engineering,” covers reservoir characterization, a huge part of the production process and crucial to the power generation supply chain. Long though of as not being “sustainable,” newly discovered sources of petroleum and newly developed methods for petroleum extraction have made it clear that not only can the petroleum industry march toward sustainability, but it can be made “greener” and more environmentally friendly. Sustainable energy engineering is where the technical, economic, and environmental aspects of energy production intersect and affect each other. This collection of papers covers the strategic and economic implications of methods used to characterize petroleum reservoirs. Born out of the journal by the same name, formerly published by Scrivener Publishing, most of the articles in this volume have been updated, and there are some new additions, as well, to keep the engineer abreast of any updates and new methods in the industry. Truly a snapshot of the state-of-the-art, this groundbreaking volume is a must-have for any petroleum engineer working in the field, environmental engineers, petroleum engineering students, and any other engineer or scientist working with reservoirs.

The book consists of a series of edited chapters, each written by an expert in the field and focusing on a particular characterization technique as applied to glass. The book covers a variety of techniques ranging from the very common (like Raman and FTIR) to the most recent (and less well known) ones, like SEM for structural analysis and photoelastic measurements. The level of the chapters make it suitable for researchers and for graduate students about to start their research work. It will also: discuss the technique itself, background, nuances when it comes to looking at glassy materials, interpretation of results, case studies, and recent and near-future innovations Fill a widening gap in modern techniques for glass characterization Provide much needed updates on the multiple essential characterization techniques

Detailed, up-to-date coverage of hazardous materials and situations Lack of awareness about hazardous materials poses a major problem, causing many needless injuries and losses of property. Incomplete awareness presents just as big a problem; often people who have contact with such materials know just enough to feel safe while actually putting themselves and others in great danger. Though regulatory agencies have provided written standards, rarely do these on their own offer the commonsense advice needed to properly evaluate and handle hazardous materials. Hazardous Materials Characterization: Evaluation Methods, Procedures, and Considerations provides detailed coverage of hazardous materials and situations. Plain language and a common- sense approach make this an accessible resource for use by all workers who handle and deal with these materials. Written according to the latest regulations and best practices, this guide groups related materials together for quick and easy access (corrosive, ignitable, radioactive, etc.). It also details methods and procedures for evaluating the properties and strengths of questionable materials, as well as what reactive substances and situations to look out for when working with these materials. Other topics covered include: * Regulatory review * Sampling and monitoring equipment, applications, and procedures * Human health hazards * Biological hazards * Radiation hazards * Evaluating chemical and biological terrorist threats * Environmental remediation methods * References and resources Packed with the most up-to-date information on hazardous materials and written to maximize accessibility, Hazardous Materials Characterization is a vital reference for all those whose work involves hazardous materials.

The definitive guide to the myriad analytical techniques available to scientists involved in biotherapeutics research Analytical Characterization of Biotherapeutics covers all current and emerging analytical tools and techniques used for the characterization of therapeutic proteins and antigen reagents. From basic recombinant antigen and antibody characterization, to complex analyses for increasingly complex molecular designs, the book explores the history of the analysis techniques and offers valuable insights into the most important emerging analytical solutions. In addition, it frames critical questions warranting attention in the design and delivery of a therapeutic protein, exposes analytical challenges that may occur when characterizing these molecules, and presents a number of tested solutions. The first single-volume guide of its kind, Analytical Characterization of Biotherapeutics brings together contributions from scientists at the leading edge of biotherapeutics research and manufacturing. Key topics covered in-depth include the structural characterization of recombinant proteins and antibodies, antibody de novo sequencing, characterization of antibody drug conjugates, characterization of bi-specific or other hybrid molecules, characterization of manufacturing host-cell contaminant proteins, analytical tools for biologics molecular assessment, and more. Each chapter is written by a recognized expert or experts in their field who discuss current and cutting edge approaches to fully characterizing biotherapeutic proteins and antigen reagents Covers the full range of characterization strategies for large molecule based therapeutics Provides an up-to-date account of the latest approaches used for large molecule characterization Chapters cover the background needed to understand the challenges at hand, solutions to characterize these large molecules, and a summary of emerging options for analytical characterization Analytical Characterization of Biotherapeutics is an up-to-date resource for analytical scientists, biologists, and mass spectrometrists involved in the analysis of biomolecules, as well as scientists employed in the pharmaceuticals and biotechnology industries. Graduate students in biology and analytical science, and their instructors will find it to be fascinating and instructive supplementary reading.

Microstructural characterization is usually achieved by allowing some form of probe to interact with a carefully prepared specimen. The most commonly used probes are visible light, X-ray radiation, a high-energy electron beam, or a sharp, flexible needle. These four types of probe form the basis for optical microscopy, X-ray diffraction, electron microscopy, and scanning probe microscopy. Microstructural Characterization of Materials, 2nd Edition is an introduction to the expertise involved in assessing the microstructure of engineering materials and to the experimental methods used for this purpose. Similar to the first edition, this 2nd edition explores the methodology of materials characterization under the three headings of crystal structure, microstructural morphology, and microanalysis. The principal methods of characterization, including diffraction analysis, optical microscopy, electron microscopy, and chemical microanalytical techniques are treated both qualitatively and quantitatively. An additional chapter has been added to the new edition to cover surface probe microscopy, and there are new sections on digital image recording and analysis, orientation imaging microscopy, focused ion-beam instruments, atom-probe microscopy, and 3-D image reconstruction. As well as being fully updated, this second edition also includes revised and expanded examples and exercises, with a solutions manual available at http://develop.wiley.co.uk/microstructural2e/ Microstructural Characterization of Materials, 2nd Edition will appeal to senior undergraduate and graduate students of material science, materials engineering, and materials chemistry, as well as to qualified engineers and more advanced researchers, who will find the book a useful and comprehensive general reference source.