Reactive Distillation Design and Control

Hands-on guidance for the design, control, and operation of azeotropic distillation systems Following this book's step-by-step guidance, readers learn to master tested and proven methods to overcome a major problem in chemical processing: the distillation and separation of azeotropes. Practical in focus, the book fully details the design, control, and operation of azeotropic distillation systems, using rigorous steady-state and dynamic simulation tools. Design and Control of Distillation Systems for Separating Azeotropes is divided into five parts: Fundamentals and tools Separations without adding other components Separations using light entrainer (heterogeneous azeotropic distillation) Separations using heavy entrainer (extractive distillation) Other ways for separating azeotropes The distillation methods presented cover a variety of important industrial chemical systems, including the processing of biofuels. For most of these chemical systems, the authors explain how to achieve economically optimum steady-state designs. Moreover, readers learn how to implement practical control structures that provide effective load rejection to manage disturbances in throughput and feed composition. Trade-offs between steady-state energy savings and dynamic controllability are discussed, helping readers design and implement the distillation system that best meets their particular needs. In addition, economic and dynamic comparisons between alternative methods are presented, including an example of azeotropic distillation versus extractive distillation for the isopropanol/water system. With its focus on practical solutions, Design and Control of Distillation Systems for Separating Azeotropes is ideal for engineers facing a broad range of azeotropic separation problems. Moreover, this book is recommended as a supplemental text for undergraduate and graduate engineering courses in design, control, mass transfer, and bio-processing.

Learn to Design the Best Control Configuration for Any Distillation Column Today, distillation is by far the most common separation technique used in the chemical and petroleum industries. All distillation columns need to be carefully controlled in order to meet specified production and quality levels. Distillation Control enables readers to do this by approaching the subject from a process to develop, analyze, and troubleshoot all aspects of column controls. Readers are efficiency and effectiveness and minimizing coats. Distillation Control begins with a chapter dedicated to underlying principles, including separation processes, reflux and boilup ratios, and composition dynamics. Next, the author covers such critical topics as: Composition control Pressure control and condensers Reboilers and feed preheaters Application of feedforward Unit optimization Complex towers As readers progress through the text, they’ll discover that the best control configuration for a distillation column is largely determined using steady-state process characteristics. The stage-by-stage separation models that the author sets forth for column design, therefore, provide information that is essential in developing the optimal control configuration. In addition to its clear explanations, Distillation Control is filled with clear diagrams and illustrations that clarify complex concepts and guide readers through multi-step procedures. Engineers as well as other professionals working in process facilities that use distillation to separate materials will fin that this book enables them to implement the latest tested and proven distillation control methods to meet their particular processing needs.

This book addresses principles and practical applications of membrane distillation and osmotic distillation, separation technologies which are gaining increasing attention due to their advantages over conventional concentration processes. • Addresses membrane and osmotic distillation, two closely related and novel processes that offer several advantages over conventional concentration processes • Has a widespread impact and application of the technology in industries such as food, environment, and nuclear clean-up / containment • Covers theoretical aspects of both processes, the properties of hydrophobic membranes, process economics, integrated processes and future prospects. • Caters the presentation caters for the diversity of readership with respect to links with membrane technologies.

Chemical Reactor Design and Control uses process simulators like Matlab®, Aspen Plus, and Aspen Dynamics to study the design of chemical reactors and their dynamic control. There are numerous books that focus on steady-state reactor design. There are no books that consider practical control systems for real industrial reactors. This unique reference addresses the simultaneous design and control of chemical reactors. After a discussion of reactor basics, it: Covers three types of classical reactors: continuous stirred tank (CSTR), batch, and tubular plug flow Emphasizes temperature control and the critical impact of steady-state design on the dynamics and stability of reactors Covers chemical reactors and control problems in a plantwide environment Incorporates numerous tables and shows step-by-step calculations with equations Discusses how to use process simulators to address diverse issues and types of operations This is a practical reference for chemical engineering professionals in the process industries, professionals who work with chemical reactors, and students in undergraduate and graduate reactor design, process control, and plant design courses.

A comprehensive treatment of model-based fuzzy control systems This volume offers full coverage of the systematic framework for the stability and design of nonlinear fuzzy control systems. Building on the Takagi-Sugeno fuzzy model, authors Tanaka and Wang address a number of important issues in fuzzy control systems, including stability analysis, systematic design procedures, incorporation of performance specifications, numerical implementations, and practical applications. Issues that have not been fully treated in existing texts, such as stability analysis, systematic design, and performance analysis, are crucial to the validity and applicability of fuzzy control methodology. Fuzzy Control Systems Design and Analysis addresses these issues in the framework of parallel distributed compensation, a controller structure devised in accordance with the fuzzy model. This balanced treatment features an overview of fuzzy control, modeling, and stability analysis, as well as a section on the use of linear matrix inequalities (LMI) as an approach to fuzzy design and control. It also covers advanced topics in model-based fuzzy control systems, including modeling and control of chaotic systems. Later sections offer practical examples in the form of detailed theoretical and experimental studies of fuzzy control in robotic systems and a discussion of future directions in the field. Fuzzy Control Systems Design and Analysis offers an advanced treatment of fuzzy control that makes a useful reference for researchers and a reliable text for advanced graduate students in the field.

THE FIRST BOOK OF ITS KIND ON DISTILLATION TECHNOLOGY The last half-century of research on distillation has tremendously improved our understanding and design of industrial distillation equipment and systems. High-speed computers have taken over the design, control, and operation of towers. Invention and innovation in tower internals have greatly enhanced tower capacity and efficiency. With all these advances, one would expect the failure rate in distillation towers to be on the decline. In fact, the opposite is the case: the tower failure rate is on the rise and accelerating. Distillation Troubleshooting collects invaluable hands-on experiences acquired in dealing with distillation and absorption malfunctions, making them readily accessible for those engaged in solving today's problems and avoiding tomorrow's. The first book of its kind on the distillation industry, the practical lessons it offers are a must for those seeking the elusive path to trouble-free distillation. Distillation Troubleshooting covers over 1,200 case histories of problems, diagnoses, solutions, and key lessons. Coverage includes: * Successful and unsuccessful struggles with plugging, fouling, and coking * Histories and prevention of tray, packing, and internals damage * Lessons taught by incidents and accidents during shutdowns, commissioning, and abnormal operation * Troubleshooting distillation simulations to match the real world * Making packing liquid distributors work * Plant bottlenecks from intermediate draws, chimney trays, and feed points * Histories of and key lessons from explosions and fires in distillation towers * Prevention of flaws that impair reboiler and condenser performance * Destabilization of tower control systems and how to correct it * Discoveries from shutdown inspections * Suppression of foam and accumulation incidents A unique resource for improving the foremost industrial separation process, Distillation Troubleshooting transforms decades of hands-on experiences into a handy reference for professionals and students involved in the operation, design, study, improvement, and management of large-scale distillation.

Distillation has historically been the main method for separating mixtures in the chemical process industry. However, despite the flexibility and widespread use of distillation processes, they still remain extremely energy inefficient. Increased optimization and novel distillation concepts can deliver substantial benefits, not just in terms of significantly lower energy use, but also in reducing capital investment and improving eco-efficiency. While likely to remain the separation technology of choice for the next few decades, there is no doubt that distillation technologies need to make radical changes in order to meet the demands of the energy-conscious society. Advanced Distillation Technologies: Design, Control and Applications gives a deep and broad insight into integrated separations using non-conventional arrangements, including both current and upcoming process intensification technologies. It includes: Key concepts in distillation technology Principles of design, control, sizing and economics of distillation Dividing-wall column (DWC) – design, configurations, optimal operation and energy efficient and advanced control DWC applications in ternary separations, azeotropic, extractive and reactive distillation Heat integrated distillation column (HIDiC) – design, equipment and configurations Heat-pump assisted applications (MVR, TVR, AHP, CHRP, TAHP and others) Cyclic distillation technology – concepts, modeling approach, design and control issues Reactive distillation – fundamentals, equipment, applications, feasibility scheme Results of rigorous simulations in Mathworks Matlab & Simulink, Aspen Plus, Dynamics and Custom Modeler Containing abundant examples and industrial case studies, this is a unique resource that tackles the most advanced distillation technologies – all the way from the conceptual design to practical implementation. The author of Advanced Distillation Technologies, Dr. Ir. Anton A. Kiss, has been awarded the Hoogewerff Jongerenprijs 2013. Find out more (website in Dutch)…

Most existing robust design books address design for static systems, or achieve robust design from experimental data via the Taguchi method. Little work considers model information for robust design particularly for the dynamic system. This book covers robust design for both static and dynamic systems using the nominal model information or the hybrid model/data information, and also integrates design with control under a large operating region. This design can handle strong nonlinearity and more uncertainties from model and parameters.

Process vent header collection systems are subject to continually varying compositions and flow rates and thus present significant challenges for safe design. Due to increasingly demanding safety, health, environmental, and property protection requirements, today's industrial designers are faced with the need to create increasingly complex systems for more effective treatment, dispersal, or disposal of process gases. Safe Design and Operation of Process Vents and Emission Control Systems provides cutting-edgeguidance for the design, evaluation, and operation of these systems, with emphasis on: Preventing fires, explosions, and toxic releases Maintaining safe vent conditions Understanding normal process operations, such as intentional routine controlled venting and emergency operations, like overpressure relief Mitigating the impacts of end-of-line treatment devices, such as scrubbers, flares, and thermal oxidizers, on the vent header system Complying with regulations Written by a team of process safety experts from the chemical, pharmaceutical, and petroleum industries, the book includes a wealth of real-world examples and a thorough overview of the tools and methods used in the profession.

Covers PID control systems from the very basics to the advanced topics This book covers the design, implementation and automatic tuning of PID control systems with operational constraints. It provides students, researchers, and industrial practitioners with everything they need to know about PID control systems—from classical tuning rules and model-based design to constraints, automatic tuning, cascade control, and gain scheduled control.  PID Control System Design and Automatic Tuning using MATLAB /Simulink introduces PID control system structures, sensitivity analysis, PID control design, implementation with constraints, disturbance observer-based PID control, gain scheduled PID control systems, cascade PID control systems, PID control design for complex systems, automatic tuning and applications of PID control to unmanned aerial vehicles. It also presents resonant control systems relevant to many engineering applications. The implementation of PID control and resonant control highlights how to deal with operational constraints. Provides unique coverage of PID Control of unmanned aerial vehicles (UAVs), including mathematical models of multi-rotor UAVs, control strategies of UAVs, and automatic tuning of PID controllers for UAVs Provides detailed descriptions of automatic tuning of PID control systems, including relay feedback control systems, frequency response estimation, Monte-Carlo simulation studies, PID controller design using frequency domain information, and MATLAB/Simulink simulation and implementation programs for automatic tuning Includes 15 MATLAB/Simulink tutorials, in a step-by-step manner, to illustrate the design, simulation, implementation and automatic tuning of PID control systems Assists lecturers, teaching assistants, students, and other readers to learn PID control with constraints and apply the control theory to various areas. Accompanying website includes lecture slides and MATLAB/ Simulink programs PID Control System Design and Automatic Tuning using MATLAB/Simulink is intended for undergraduate electrical, chemical, mechanical, and aerospace engineering students, and will greatly benefit postgraduate students, researchers, and industrial personnel who work with control systems and their applications.